Microwave Chemistry in Organic Synthesis (By A. Bacher ...
6 The Knoevenagel condensation of benzaldehyde and malonic acid employing piperidine as base catalyst at 140 oC for 10 min affords a yield of 85 % (5 mmol) and 86 % (0.5 mol) in different scales. However, it is important to note that the pressure in the system increased significantly due to the formation of carbon dioxide (conventional: 85 o
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